2,3,5,6-四氟三氟甲苯合成路线 （共 27 条）
反应条件
4-(N,N-dimethlyamino)pyridine; C21H27AuN2 in dichloromethane T=40°C; 12 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 134, # 39 p. 16216 - 16227,12
反应条件
water; phosphorous acid trisdiethylamide in N,N-dimethyl-formamide T=20°C; protodebromination; 0.25 h;
参考文献
Russian Chemical Bulletin, , vol. 46, # 4 p. 786 - 788
反应条件
ammonium hydroxide; zinc T=20°C; Dehalogenation; 39 h;
参考文献
Journal of Fluorine Chemistry, , vol. 96, # 2 p. 175 - 185
反应条件
XeF2; cesium fluoride in acetonitrile T=10 - 20°C; 0.5 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 58, # 11 p. 2580 - 2588,2297 - 2303
反应条件
bis(1,5-cyclooctadiene)nickel (0); tributylphosphine in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) T=100°C; 8 h; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 3 p. 443 - 447
反应条件
water; phosphorous acid trisdiethylamide in N,N-dimethyl-formamide T=20°C; protodechlorination; 0.5 h;
参考文献
Russian Chemical Bulletin, , vol. 46, # 4 p. 786 - 788
参考文献
Journal of Organic Chemistry, , vol. 31, p. 746 - 749
反应条件
1: 4-chloroheptafluorotoluene With zinc in N,N-dimethyl-formamide T=135°C; 4 h; 2: 3-chloroprop-1-ene With copper(l) chloride in N,N-dimethyl-formamide Further stages.;
参考文献
Russian Journal of Organic Chemistry, , vol. 44, # 1 p. 95 - 102
参考文献
Izvestiya Sibirskogo Otdeleniya Akademii Nauk SSSR, Seriya Khimicheskikh Nauk, , # 6 p. 78 - 88
C.A., , vol. 78, p. 83964
反应条件
1-trifluoromethyl-4-methyl-2,3,5,6-tetrafluorobenzene; phosphorous acid trisdiethylamide in diethyl ether; water 22 h;
参考文献
Russian Chemical Bulletin, , vol. 46, # 8 p. 1434 - 1436
