1,4-双（溴二氟甲基）苯合成路线 （共 8 条）
反应条件
N-bromosuccinmide in tetrachloromethane HeatingIrradiation;
参考文献
Dolbier, William R.; Asghar, Mohammed Ali; Pan, He-Qi; Celewicz, Lech
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1827 - 1830
反应条件
1: 88 percent / SF4 / 150 °C 2: 78 percent / N-bromosuccinimide / CCl4 / Heating; Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1827 - 1830
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in acetonitrile
参考文献
Journal of Organic Chemistry, , vol. 28, p. 2877 - 2879
反应条件
1: 80 percent / Br2 / 5 h / 130 - 160 °C 2: 85 percent / SbF3 / 120 °C / 40 Torr 3: 55 percent / N-bromosuccinimide / CCl4 / Heating; Irradiation View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 29, # 10 p. 1663 - 1665
Zhurnal Organicheskoi Khimii, , vol. 29, # 10 p. 1999 - 2001
反应条件
1: 85 percent / SbF3 / 120 °C / 40 Torr 2: 55 percent / N-bromosuccinimide / CCl4 / Heating; Irradiation View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 29, # 10 p. 1663 - 1665
Zhurnal Organicheskoi Khimii, , vol. 29, # 10 p. 1999 - 2001
反应条件
TMS-SnBu3; cesium fluoride in tetrahydrofuran; dimethyl sulfoxide T=78°C; 28 h;
参考文献
Dolbier Jr., William R.; Duan, Jian-Xin; Roche, Alex J.
Organic Letters, 2000 , vol. 2, # 13 p. 1867 - 1869
反应条件
calcium chloride; zinc in N,N-dimethyl acetamide T=120 - 140°C; 4 h; Catalytic behavior; Reagent/catalyst;
参考文献
LIN, Chun-Hsu; SUN, Chien-Yi; YIN, Yung-Yu; LI, Chun-Shih; CHOU, Yo-Chun
Patent: US2014/11986 A1, 2014 ;
Location in patent: Paragraph 0048 ;
反应条件
lithium aluminium tetrahydride; titanium tetrachloride in tetrahydrofuran Heating;
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1827 - 1830
