1-[4-(苯磺基）苯基]乙酮合成路线 （共 17 条）
反应条件
1: in tetrahydrofuran; diethyl ether T=60°C; 0.5 h; Microwave irradiation; 2: With hydrogenchloride; water in tetrahydrofuran; diethyl ether T=100°C; 0.5 h; Microwave irradiation;
参考文献
WO2013/131018 A1, ;
Page/Page column 54; 55 ;
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in chloroform T=20°C; 48 h;
参考文献
Journal of Chemical Research, Miniprint, , # 6 p. 2201 - 2214
反应条件
copper(l) iodide; sodium (SC)-prolinate in dimethyl sulfoxide T=90°C; 48 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 7 p. 2696 - 2700
反应条件
quinoline; copper(l) chloride in 1-methyl-pyrrolidin-2-one T=140°C; 0.25 h; Microwave irradiation;
参考文献
Synlett, , # 18 p. 2750 - 2756
反应条件
1,10-phenanthroline; copper ferrite in N,N-dimethyl-formamide T=110°C; 12 h; Green chemistry;
参考文献
Advanced Synthesis and Catalysis, , vol. 356, # 4 p. 805 - 817
反应条件
in N,N-dimethyl-formamide T=125°C; 48 h;
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 11 p. 3295 - 3301
反应条件
in dimethyl sulfoxide T=130°C; 16 h;
参考文献
Journal of Organic Chemistry, , vol. 54, # 19 p. 4691 - 4692
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in chloroform T=20°C; 48 h; Further byproducts given;
参考文献
Journal of Chemical Research, Miniprint, , # 6 p. 2201 - 2214
反应条件
1.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / 160 °C 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 20 °C 3.1: tetrahydrofuran; diethyl ether / 0.5 h / 60 °C / |Microwave irradiation 3.2: 0.5 h / 100 °C / |Microwave irradiation View Scheme
反应条件
1.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / 160 °C 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 20 °C 3.1: tetrahydrofuran; diethyl ether / 0.5 h / 60 °C / |Microwave irradiation 3.2: 0.5 h / 100 °C / |Microwave irradiation View Scheme
