N-环丙基-4-甲基苯磺酰胺合成路线 （共 3 条）
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil; tetrahydrofuran / 1 h / |Inert atmosphere 1.2: |Reflux 2.1: N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine / N,N-dimethyl-formamide / 72 h / |UV-irradiation View Scheme
参考文献
O'Sullivan, Steven; Doni, Eswararao; Tuttle, Tell; Murphy, John A.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 474 - 478
Angew. Chem., 2013 , vol. 126, # 2 p. 484 - 488,5
反应条件
pyridine in water
T=20°C; 1 h;
参考文献
O'Sullivan, Steven; Doni, Eswararao; Tuttle, Tell; Murphy, John A.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 474 - 478
Angew. Chem., 2013 , vol. 126, # 2 p. 484 - 488,5
反应条件
(i) Br2, aq. NaOH, CHCl3, (ii) MeOH, CH2Cl2, (irradiation); Multistep reaction;
参考文献
Dekker; Engberts; De Boer Th.
Recueil des Travaux Chimiques des Pays Bas, 1978 , vol. 97, # 2 p. 39 - 41
