2-甲氧基苯并环庚-5-酮合成路线 (共 42 条)
反应条件
PPA in chlorobenzene T=80°C; 15 h;
参考文献
WO2012/50848 A1, ;
Page/Page column 115-116 ;
反应条件
chromium (VI) oxide; acetic acid in water T=20°C; 24 h;
参考文献
US2006/293394 A1, ;
Page/Page column 25 ;
反应条件
barium permanganate in acetonitrile 2 h; Heating;
参考文献
Tetrahedron, , vol. 46, # 19 p. 6869 - 6878
反应条件
barium permanganate in acetonitrile 5 h; Heating;
参考文献
Synthetic Communications, , vol. 19, # 20 p. 3469 - 3476
反应条件
titanium tetrachloride 18 h; 1.) -78 degC, 2.) -10 to 0 degC;
参考文献
Journal of the American Chemical Society, , vol. 106, # 8 p. 2469 - 2471
反应条件
copper diacetate; zinc in acetic acid
参考文献
Journal of the American Chemical Society, , vol. 95, p. 6655 - 6665
反应条件
1: bis-(2-methoxy-ethyl) ether 2: NaOH / methanol 3: Zn, Cu(OAc)2 / acetic acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 95, p. 6655 - 6665
反应条件
1: NaOH / methanol 2: Zn, Cu(OAc)2 / acetic acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 95, p. 6655 - 6665
反应条件
1: TsOH 2: bis-(2-methoxy-ethyl) ether 3: NaOH / methanol 4: Zn, Cu(OAc)2 / acetic acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 95, p. 6655 - 6665
反应条件
silver trifluoromethanesulfonate in dichloromethane 17 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 43, # 8 p. 1847 - 1856