5-(3-甲氧基苯基)-戊基-2,4-二烯酸合成路线 （共 4 条）
反应条件
1: 23 g / hydrogen / 10percent Pd-C / ethanol / 760 Torr / Ambient temperature 2: PCl5 / benzene / 0.5 h / Heating 3: SnCl4 / benzene / 24 h / Ambient temperature View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 20, # 2 p. 140 - 143
参考文献
Khan,A.M. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 990 - 994
反应条件
1: nickel-aluminum alloy; sodium hydroxide
2: polyphosphoric acid
3: acetic acid; bromine
4: lithium chloride / N,N-dimethyl-formamide / |Reflux
5: boron tribromide / dichloromethane / |Reflux
6: hydroxylamine hydrochloride; pyridine / ethanol
7: triethylamine / dichloromethane / 0.17 h / 0 °C
8: toluene; diethyl ether / 1.5 h / -20 - 0 °C / |Inert atmosphere
View Scheme
参考文献
Kang, Zhi-Yun; Zhang, Qing-Jian; Chen, Ruo-Yun; Zhang, Pei-Cheng; Yu, De-Quan
Journal of Asian Natural Products Research, 2013 , vol. 15, # 8 p. 840 - 848
反应条件
hydrogen; nickel in ethanol
参考文献
Lal; Khanna; Anand
Journal of medicinal chemistry, 1972 , vol. 15, # 1 p. 23 - 27
