6,8-二甲氧基-1,3-萘二醇合成路线 (共 5 条)
参考文献
Bycroft,B.W.; Roberts,J.C.
Journal of the Chemical Society, 1963 , p. 4868 - 4872
反应条件
sodium hydride in N,N-dimethyl-formamide; mineral oil
T=20°C; 1 h; Inert atmosphere;
参考文献
Pepper, Henry P.; George, Jonathan H.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 46 p. 12170 - 12173
Angew. Chem., 2013 , vol. 125, # 46 p. 12392 - 12395,4
反应条件
1: perchloric acid / 36 h / 20 °C / |Inert atmosphere
2: sodium hydride / mineral oil; N,N-dimethyl-formamide / 1 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Pepper, Henry P.; George, Jonathan H.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 46 p. 12170 - 12173
Angew. Chem., 2013 , vol. 125, # 46 p. 12392 - 12395,4
反应条件
boron tribromide in dichloromethane
6 h; Ambient temperature;
参考文献
Viviani, Fabrice; Gaudry, Michel; Marquet, Andree
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 5 p. 1255 - 1259
反应条件
iodine; magnesium in diethyl ether; benzene
参考文献
Henriques,A.T. et al.
Synthesis, 1977 , p. 713 - 716