N,N-二乙基对甲苯磺酰胺合成路线 (共 38 条)
反应条件
copper(ll) bromide in dimethyl sulfoxide T=100°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Tang, Xiaodong; Huang, Liangbin; Qi, Chaorong; Wu, Xia; Wu, Wanqing; Jiang, Huanfeng
Chemical Communications, 2013 , vol. 49, # 54 p. 6102 - 6104
反应条件
in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Schneider, Cedric; Broda, Ellen; Snieckus, Victor
Organic Letters, 2011 , vol. 13, # 14 p. 3588 - 3591
反应条件
1: 4-methylphenyl triisopropylsilyl sulfide With sulfuryl dichloride; potassium nitrate in acetonitrile T=0°C; 2: diethylamine in acetonitrile
参考文献
Gareau, Yves; Pellicelli, Jonathan; Laliberte, Sebastien; Gauvreau, Danny
Tetrahedron Letters, 2003 , vol. 44, # 42 p. 7821 - 7824
反应条件
triethylamine; triphenylphosphine in dichloromethane T=0°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 2 p. 683 - 685
反应条件
In(OSO2CF3)3 in 1,2-dichloro-ethane T=100°C; 24 h;
参考文献
Frost, Christopher G.; Hartley, Joseph P.; Griffin, David
Synlett, 2002 , # 11 p. 1928 - 1930
反应条件
triethylamine in dichloromethane T=0 - 20°C; 2.16667 h; Inert atmosphere;
参考文献
Inman, Martyn; Carbone, Anna; Moody, Christopher J.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1217 - 1232
反应条件
N-chloro-N,N-diethylamine in dichloromethane 0.5 h; Ambient temperature;
参考文献
Nishikawa; Inaba; Furukawa
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 4 p. 1374 - 1377
反应条件
N-chloro-morpholine in dichloromethane 0.5 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 4 p. 1374 - 1377
反应条件
silver tetrafluoroborate; dibromo[1,3-dihydro-1-(2-pyridinyl)-3-(2,4,6-trimethylphenyl)-2H-imidazol-2-ylidene]platinum(II) in PhNO2-d5 T=20 - 150°C; P=4125.41 Torr; 26 h; Inert atmosphere;
参考文献
Organometallics, , vol. 31, # 3 p. 921 - 929
反应条件
in tetrahydrofuran T=20 - 22°C; 111 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 39, # 1 p. 203 - 211