(3-甲氧基-4-硝基苯基)肼合成路线 （共 3 条）
反应条件
hydrazine in ethanol; water
T=20 - 100°C; 2 h;
参考文献
BIAL-PORTELA and COMPANHIA, S.A.
Patent: WO2009/84970 A1, 2009 ;
Location in patent: Page/Page column 73 ;
WO 2009/084970 A1
反应条件
1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C
1.2: 2 h / 60 °C
2.1: hydrazine hydrate / ethanol / |Reflux
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参考文献
GLENMARK PHARMACEUTICALS S.A.; GHARAT, Laxmikant Atmaram; MUTHUKAMAN, Nagarajan; KHAIRATKAR-JOSHI, Neelima; KATTIGE, Vidya Ganapati
Patent: WO2013/186692 A1, 2013 ;
反应条件
pyridine in dichloromethane
T=20°C; 2 h;
参考文献
AVENTIS PHARMA DEUTSCHLAND GMBH
Patent: WO2004/7455 A1, 2004 ;
Location in patent: Page/Page column 29 ;
