2,6-二-叔-丁基-4-氢过氧基-4-甲基-2,5-环己二烯酮合成路线 （共 19 条）
反应条件
1: NaI; acetic acid View Scheme
参考文献
Gersmann; Bickel
Journal of the Chemical Society, 1959 , p. 2711,2713
参考文献
Gersmann; Bickel
Journal of the Chemical Society, 1959 , p. 2711,2713
反应条件
triphenylphosphine in dichloromethane 3 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 12 p. 3852 - 3855
反应条件
copper(l) iodide in acetonitrile T=20°C; 1 h;
参考文献
Tetrahedron, , vol. 49, # 34 p. 7455 - 7462
反应条件
copper dichloride in acetonitrile T=20°C; 1 h;
参考文献
Tetrahedron, , vol. 49, # 34 p. 7455 - 7462
反应条件
1: pyridine / petroleum ether / 1.) 30 min, 0 deg C, 2.) 2 h, room temp. 2: 54 percent Spectr. / t-BuOK / petroleum ether; dimethylformamide / 2 h / -60 °C View Scheme
参考文献
Nishinaga, Akira; Nakamura, Koichi; Matsuura, Teruo
Journal of Organic Chemistry, 1983 , vol. 48, # 21 p. 3696 - 3700
反应条件
lt;Co(CN)5O2gt;(3-)*3Et4N(1+); oxygen in N,N-dimethyl-formamide
T=0°C; 2 h;
参考文献
Nishinaga, A.; Tomita, H.; Matsuura, T.
Tetrahedron Letters, 1980 , vol. 21, p. 2833 - 2836
反应条件
potassium hydroxide; oxygen
参考文献
Kharasch; Joshi
Journal of Organic Chemistry, 1957 , vol. 22, p. 1439,1442
Show Details
Gersmann; Bickel
Journal of the Chemical Society, 1959 , p. 2711,2713
反应条件
C5CoN5O2(3-)*3C36H30NP2(1+) in dichloromethane
T=-70°C; 0.0833333 h; starting material added in dimer form; Title compound not separated from byproducts;
参考文献
Nishinaga, A.; Tomita, H.; Matsuura, T.
Tetrahedron Letters, 1980 , vol. 21, p. 3407 - 3408
反应条件
dihydrogen peroxide; 12-molybdophosphoric acid HPMo in acetic acid
T=30°C; 5 h; other heteropolyacids as catalyst; Product distribution;
参考文献
Shimizu, Masao; Orita, Hideo; Hayakawa, Takashi; Watanabe, Yoshihito; Takehira, Katsuomi
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 6 p. 1835 - 1837
