4-甲基苯硫代亚磺酸 S-(4-甲基苯基)酯合成路线 （共 36 条）
反应条件
sodium methylate in tetrahydrofuran T=0°C; 2 h; Yields of byproduct given;
参考文献
Bulletin de la Societe Chimique de France, , vol. 133, # 11 p. 1127 - 1141
反应条件
in chloroform-d1 2 h; Ambient temperature; Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 37, # 50 p. 9101 - 9104
反应条件
benzenesulfenyl chloride in chloroform-d1 T=-10°C; Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 37, # 50 p. 9101 - 9104
反应条件
in chloroform 16 h; Ambient temperature;
参考文献
Gazzetta Chimica Italiana, , vol. 120, # 7 p. 421 - 426
反应条件
1: 7.75 g / sodium p-toluenesulfinate / dimethylformamide / 24 h / 75 °C 2: 92.5 percent / sodium p-toluenesulfinate / dimethylformamide / 24 h / Heating View Scheme
参考文献
Acta Chimica Academiae Scientiarum Hungaricae, , vol. 106, # 4 p. 275 - 284
反应条件
in chloroform-d1 T=-10°C; Yield given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 37, # 50 p. 9101 - 9104
反应条件
p-toluenesulfinic acid sodium salt in N,N-dimethyl-formamide T=75°C; 24 h;
参考文献
Acta Chimica Academiae Scientiarum Hungaricae, , vol. 106, # 4 p. 275 - 284
反应条件
18-crown-6 ether 1.) pyridine, 0 deg C, 30 min; 2.) HCl, H2O; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 37, p. 37 - 44
反应条件
18-crown-6 ether 1.) pyridine, 0 deg C, 30 min; 2.) H2O-MeOH, overnight, room temp.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 37, p. 37 - 44
反应条件
in chloroform-d1 192 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 37, # 50 p. 9101 - 9104
