1-氯-3-巯基-2-丙醇合成路线 （共 5 条）
参考文献
Sjoeberg
Svensk Kemisk Tidskrift, 1938 , vol. 50, p. 253
Chem. Zentralbl., 1939 , vol. 110, # I p. 2756
参考文献
Sjoeberg
Svensk Kemisk Tidskrift, 1938 , vol. 50, p. 253
Chem. Zentralbl., 1939 , vol. 110, # I p. 2756
反应条件
bis(trimethylsilyl)-sulfide; tetrabutyl ammonium fluoride in tetrahydrofuran
T=-20°C; 0.5 h;
参考文献
GE HEALTHCARE LIMITED; MEDI-PHYSICS, INC.; NEWINGTON, Ian, Martin; WYNN, Duncan George; NAIRNE, Robert James Domett; GUILBERT, Benedicte; MANDAL, Subrata; JINTO, Jose; VARADARAJAN, Sunderaraman; RANGASWAMY, Chitralekha; BETTS, Helen; DAVIS, Rebecca
Patent: WO2011/150183 A1, 2011 ;
Location in patent: Page/Page column 194 ;
WO 2011/150183 A1
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=-15°C;
参考文献
Degl'Innocenti, Alessandro; Capperucci, Antonella; Cerreti, Arianna; Pollicino, Salvatore; Scapecchi, Serena; Malesci, Irene; Castagnoli, Giulio
Synlett, 2005 , # 20 art. no. G29005ST, p. 3063 - 3066
反应条件
iodine; sodium hydrogencarbonate in water
参考文献
Cossar,B.C.; Reynolds,D.D.
Journal of Heterocyclic Chemistry, 1965 , vol. 2, p. 430 - 440
