1.1: toluene / 4 h / 80 °C / Inert atmosphere
2.1: n-butyllithium / diethyl ether; hexane / 1 h / 0 °C / Inert atmosphere
2.2: 1 h / 20 °C / Inert atmosphere
3.1: formic acid / 0.5 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Gellrich, Urs; Huang, Jing; Seiche, Wolfgang; Keller, Manfred; Meuwly, Markus; Breit, Bernhard
Journal of the American Chemical Society, 2011 , vol. 133, # 4 p. 964 - 975
1.1: n-butyllithium / diethyl ether; hexane / 1 h / 0 °C / Inert atmosphere
1.2: 1 h / 20 °C / Inert atmosphere
2.1: formic acid / 0.5 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Gellrich, Urs; Huang, Jing; Seiche, Wolfgang; Keller, Manfred; Meuwly, Markus; Breit, Bernhard
Journal of the American Chemical Society, 2011 , vol. 133, # 4 p. 964 - 975