1-(2-烯丙基苯基)乙酮合成路线 (共 3 条)
反应条件
1: LDA / tetrahydrofuran; hexane / 2 h / -78 °C 2: (PCy3)Cl2Ru(=CHPh)[-CHN(Mes)CH2CH2N(Mes)-] / benzene / 1 h / 65 °C View Scheme
参考文献
Okada, Akihiro; Ohshima, Takashi; Shibasaki, Masakatsu
Tetrahedron Letters, 2001 , vol. 42, # 45 p. 8023 - 8027
反应条件
1.1: hydroxylamine hydrochloride / pyridine
1.2: triethylamine
2.1: 77 percent / triethylamine; (n-Bu)4NCl / Pd(PPH3)4 / dimethylformamide / 4 h / 80 °C
View Scheme
参考文献
Tsutsui, Hironori; Narasaka, Koichi
Chemistry Letters, 2001 , # 6 p. 526 - 527
反应条件
hydrogenchloride; Cp2Ti(PMe3)2; (Ph)2SiH2; trimethylphosphane
Yield given. Multistep reaction;
参考文献
Kablaoui, Natasha M.; Buchwald, Stephen L.
Journal of the American Chemical Society, 1996 , vol. 118, # 13 p. 3182 - 3191