1,1,1-三氟-2-(三氟甲基)-4-戊-2-醇合成路线 （共 8 条）
参考文献
Journal of Organic Chemistry, , vol. 32, p. 347 - 352
参考文献
Journal of Organic Chemistry, , vol. 33, p. 2302 - 2310
反应条件
(i), (ii) (HOCH2CH2)3N; Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 154, p. 131 - 145
反应条件
1: With sulfuric acid in water T=0 - 25°C; 2 h; 2: With water T=90 - 95°C; 2 h;
参考文献
Central Glass Company, Ltd.
Patent: US2005/165249 A1, 2005 ;
Location in patent: Page/Page column 4 ;
反应条件
1: With dimethylsulfide borane complex in tetrahydrofuran T=15 - 20°C; 48 h; 2: With sodium hydroxide in tetrahydrofuran; water 3: With dihydrogen peroxide in tetrahydrofuran; water T=20°C;
参考文献
ST-JEAN PHOTOCHIMIE INC.; INTERNATIONAL BUSINESS MACHINES CORPORATION (IBM)
Patent: WO2006/50609 A1, 2006 ;
Location in patent: Page/Page column 14-15 ;
反应条件
Diels-Alder reaction; Heating;
参考文献
Ishikawa, Takuji; Kodani, Tesuhiro; Yoshida, Tomohiro; Moriya, Tsukasa; Yamashita, Tsuneo; Toriumi, Minoru; Araki, Takayuki; Aoyama, Hirokazu; Hagiwara, Takuya; Furukawa, Takamitsu; Itani, Toshiro; Fujii, Kiyoshi
Journal of Fluorine Chemistry, 2004 , vol. 125, # 11 SPEC. ISS. p. 1791 - 1799
反应条件
tris-(trifluoromethanesulfonyl)methane acid
T=110°C; 7 h;
参考文献
Central Glass Company, Limited
Patent: US2012/4444 A1, 2012 ;
Location in patent: Page/Page column 6-7 ;
反应条件
1: With dimethylsulfide borane complex in tetrahydrofuran
T=15 - 20°C; 48 h;
2: With sodium hydroxide in tetrahydrofuran; water
3: With dihydrogen peroxide in tetrahydrofuran; water
T=20°C;
参考文献
ST-JEAN PHOTOCHIMIE INC.; INTERNATIONAL BUSINESS MACHINES CORPORATION (IBM)
Patent: WO2006/50609 A1, 2006 ;
Location in patent: Page/Page column 14-15 ;
