(R)-(-)-4-烯基-2-戊醇合成路线 (共 30 条)
反应条件
1: in diethyl ether; pentane T=-100°C; 1 h; 2: With sodium hydroxide; dihydrogen peroxide in methanol Further stages. Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 66, # 7 p. 2512 - 2514
反应条件
acidic phthalic acid ester; brucine salt of hydrogenphthalate
参考文献
Journal of Biological Chemistry, , vol. 81, p. 427
Science (Washington, DC, United States), vol. 69, p. 47
Chem. Zentralbl., , vol. 100, # I p. 1211
反应条件
whole lyophilised cells of Rhodococcus ruber DSM; acetone in phosphate buffer T=30°C; pH=8.0; 38 h;
参考文献
Tetrahedron Asymmetry, , vol. 14, # 2 p. 275 - 280
参考文献
WO2006/53039 A2, ;
Page/Page column 42 ;
反应条件
ammonia; sodium in tetrahydrofuran
参考文献
Chemistry--A European Journal, , vol. 2, # 9 p. 1164 - 1172
反应条件
in diethyl ether T=-78°C; 7 h; Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 343, # 1 p. 89 - 94
反应条件
(dimethyl)chloroborane Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 105, # 7 p. 2092 - 2098
反应条件
CALB in various solvent(s) T=30°C; 1 h; Product distribution; Further Variations:ReagentsTemperaturestime;
参考文献
Organic and biomolecular chemistry, , vol. 2, # 14 p. 2050 - 2060
反应条件
triethanolamine 1.) propane, -90 deg C, 2 h; 12 h, 20 deg C, 2.) 2 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 114, # 1 p. 359 - 374
反应条件
triethanolamine 1.) propane, -90 deg C, 2 h; 12 h, 20 deg C, 2.) 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 114, # 1 p. 359 - 374