2-溴-4-甲氧基-5-苄氧基苯甲醛合成路线 （共 22 条）
反应条件
potassium carbonate in acetone 4 h; Heating;
参考文献
Chandrasekhar; Reddy, N. Ramakrishna; Rao, Y. Srinivasa
Tetrahedron, 2006 , vol. 62, # 51 p. 12098 - 12107
反应条件
1: 41.3 g / K2CO3 / acetonitrile / 1 h / Heating 2: 45.4 g / bromine / methanol; CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 22 p. 7136 - 7137
反应条件
potassium carbonate T=100°C; 6 h;
参考文献
Imakura, Yasuhiro; Okimoto, Kazuto; Gorohata, Chizuru; Kobayashi, Shigeru; Kihara, Masaru; Yamashita, Shinsuke
Heterocycles, 1990 , vol. 31, # 6 p. 1067 - 1076
反应条件
bromine in methanol T=25 - 35°C; 1 h;
参考文献
Reddy, Jambula Mukunda; Kumar, Kotagiri Vijay; Raju, Veeramalla; Bhaskar, Bolguddu Vijay; Himabindu, Vurumidi; Bhattacharya, Apurba; Sundaram, Venkatram; Banerjee, Rahul; Reddy, Ghanta Mahesh; Bandichhor, Rakeshwar
Synthetic Communications, 2008 , vol. 38, # 13 p. 2138 - 2149
反应条件
1: 41.3 g / K2CO3 / acetonitrile / 1 h / Heating 2: 45.4 g / bromine / methanol; CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 22 p. 7136 - 7137
反应条件
sodium hydroxide T=85°C; 1 h;
参考文献
Imakura, Yasuhiro; Okimoto, Kazuto; Gorohata, Chizuru; Kobayashi, Shigeru; Kihara, Masaru; Yamashita, Shinsuke
Heterocycles, 1990 , vol. 31, # 6 p. 1067 - 1076
反应条件
1: 85 percent / sulfuric acid / 6 h / 90 °C 2: 90 percent / potassium carbonate / acetone / 4 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 62, # 51 p. 12098 - 12107
反应条件
1: 91 percent / bromine / methanol / 1 h / cooling 2: 85 percent / sulfuric acid / 6 h / 90 °C 3: 90 percent / potassium carbonate / acetone / 4 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 62, # 51 p. 12098 - 12107
反应条件
1: 100 percent / K2CO3 / dimethylformamide / 50 °C 2: 79 percent / Br2 / dimethylformamide View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 47, # 10 p. 1512 - 1513
反应条件
1: potassium bromide; bromine / water / 20 °C 2: hydrogenchloride / water / 10 h / 90 °C 3: ethanol / 18 h / |Reflux View Scheme
参考文献
Journal of the American Chemical Society, , vol. 136, # 6 p. 2583 - 2591
