3,7,11,15-四甲基十六烷-1-醇合成路线 （共 20 条）
反应条件
sodium bissulfite; chromic acid; acetic acid in hexadeuterioacetone; water
参考文献
Hirai, Kunihiro; Katayama, Satoshi; Torii, Takayoshi; Nakaya, Ryotaro; Takahashi, Daisuke
Patent: US2013/267697 A1, 2013 ;
Location in patent: Page/Page column ;
反应条件
soda lime T=260 - 280°C;
参考文献
Karrer; Epprecht; Koenig
Helvetica Chimica Acta, vol. 23, p. 280
反应条件
n-octadecanoic acid chloride T=125°C; und Zersetzen des entstandenen Esters bei 420grad;
参考文献
Karrer; Helfenstein; Widmer
Helvetica Chimica Acta, 1928 , vol. 11, p. 1206
反应条件
T=320°C; Decomposition; 5 h;
参考文献
Chemistry Letters, , # 3 p. 206 - 207
反应条件
hydrogen iodide T=70 - 80°C;
参考文献
Kuhn; Suginome
Helvetica Chimica Acta, 1929 , vol. 12, p. 916
反应条件
1: acetic acid; chromic acid; sodium bissulfite / water; hexadeuterioacetone 2: thionyl chloride / chloroform View Scheme
参考文献
Hirai, Kunihiro; Katayama, Satoshi; Torii, Takayoshi; Nakaya, Ryotaro; Takahashi, Daisuke
Patent: US2013/267697 A1, 2013 ;
反应条件
T=320°C; Decomposition; 5 h;
参考文献
Chemistry Letters, , # 3 p. 206 - 207
反应条件
hydrogen in ethanol
T=20°C; P=760.051 Torr; 2 h;
参考文献
Cayla; Vernejoul, Fabienne; Debin, Arnaud; Drocourt, Daniel; Perouzel, Eric; Tiraby, Gérard; Lioux, Thierry
Patent: EP2674170 A1, 2013 ;
Location in patent: Paragraph 0151 ;
反应条件
hydrogen; sodium hydrogencarbonate; platinum(IV) oxide in tetrahydrofuran
P=760.051 Torr; 20 h;
参考文献
CHIMERIX, INC.; UNIVERSITY OF CALIFORNIA, SAN DIEGO
Patent: WO2007/130783 A2, 2007 ;
Location in patent: Page/Page column 29-30 ;
参考文献
Nisshin Flour Milling Co., Ltd.
Patent: US4221810 A1, 1980 ;
