in methanol; toluene Cu(CH3CN)4PF6 dissolved in MeOH added to CdS in toluene; washed with MeOH, centrifuged; monitored by XRD;

in chloroform byproducts: CuCl; (N2); Schlenk technique; mixt. of Ti complex and Cu complex in CHCl3 wasstirred for 3 h; dried (vac.); residue extd. (CHCl3); filtered; filtrate dried (vac.); elem. anal.;

in dichloromethane; water; acetonitrile 12 h; Inert atmosphereSchlenk technique;

in dichloromethane

in dichloromethane (N2); elem. anal.;