3,4,5-三甲氧基甲苯合成路线 （共 96 条）
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 2.) -78 deg C; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 12, # 1 p. 49 - 52
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 25 min, 2.) -78 deg C, 10 min; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 12, # 1 p. 49 - 52
参考文献
Chemische Berichte, , vol. 26, p. 2019
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 15B, p. 18 - 20
参考文献
Journal of Organic Chemistry, , vol. 59, # 19 p. 5587 - 5595
反应条件
(i) Zn-Hg, HCl, (ii) /BRN= 635994/, OH-; Multistep reaction;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 28, p. 453 - 464
反应条件
(i) LiAlH4, THF, (ii) /BRN= 635994/, aq. NaOH; Multistep reaction;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 763, p. 109 - 120
反应条件
1: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; potassium tert-butylate in tetrahydrofuran T=-78°C; 0.25 h; Inert atmosphere; 2: With ethylene dibromide in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; regioselective reaction;
参考文献
Blangetti, Marco; Fleming, Patricia; O'Shea, Donal F.
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2870 - 2877
反应条件
1: 47 percent / 30percent H2O2, HOAc / 192 h / Ambient temperature 2: 92.1 percent / NaBH4 / H2O; diethyl ether; methanol / 0.25 h / Ambient temperature View Scheme
参考文献
Carpino, Louis A.; Triolo, Salvatore A; Berglund, Richard A
Journal of Organic Chemistry, 1989 , vol. 54, # 14 p. 3303 - 3310
反应条件
sulfuric acid; 3,3-dimethyldioxirane in acetone T=20°C; 2 h;
参考文献
Adam; Shimizu
Synthesis, 1994 , # 6 p. 560 - 562
