1: With 2,6-di-tert-butyl-4-methyl-phenol
T=-78 - 20°C; Inert atmosphereSealed tubeDarkness;
2: With water
参考文献
O'Brien, Christopher J.; Lavigne, Florie; Coyle, Emma E.; Holohan, Andrew J.; Doonan, Bryan J.
Chemistry - A European Journal, 2013 , vol. 19, # 19 p. 5854 - 5858
1: With sodium in toluene
T=105°C;
2: With chlorobenzene in toluene
T=45 - 50°C;
3: phenylphosphonous dichloride; 2,4,6-trimethylbenzoyl chloride With water; butan-1-ol
more than 3 stages;