4-(2-氨基乙基)苯甲醇合成路线 (共 6 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C;
参考文献
US2006/25400 A1, ;
Page/Page column 54 ;
US 20060025400 A1
反应条件
diborane in tetrahydrofuran 10 h; Heating;
参考文献
Behr, Jean-Paul; Lehn, Jean-Marie
Helvetica Chimica Acta, 1980 , vol. 63, # 7 p. 2112 - 2118
反应条件
1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 3 h / Inert atmosphere; Reflux; Irradiation 2: methanol; water / 5 h / Inert atmosphere; Reflux 3: lithium aluminium tetrahydride; AlCl3, aluminium chloride / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 5 p. 1383 - 1400
反应条件
1: methanol; water / 5 h / Inert atmosphere; Reflux 2: lithium aluminium tetrahydride; AlCl3, aluminium chloride / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 5 p. 1383 - 1400
反应条件
hydrogenchloride; potassium cyanide in tetrahydrofuran; methanol; water
参考文献
Naleway, John J.; Jiang, Ying; Link-Cole, Ryan
Patent: US2013/150254 A1, 2013 ;
Location in patent: Page/Page column ;