3-硝基-1,5-萘啶-2(1H)-酮合成路线 （共 5 条）
反应条件
1: PCl5; POCl3 2: palladium; methanol / Hydrogenation View Scheme
参考文献
Schering A.G.
Patent: DE700862 , 1938 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Schering Corp.
Patent: US2226111 , 1939 ;
反应条件
trichlorophosphate
15 h; Heating;
参考文献
Wozniak, M.; Plas, H. C. van der; Tomula, M.; Veldhuizen, A. van
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, p. 511 - 513
反应条件
phosphorus pentachloride; trichlorophosphate
T=135°C; 2.5 h; Yield given. Yields of byproduct given;
参考文献
Wozniak, M.; Plas, H. C. van der; Tomula, M.; Veldhuizen, A. van
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, p. 511 - 513
反应条件
1: 60 percent / phosphoryl chloride / 15 h / Heating
2: 32 percent / potassium permanganate / liquid ammonia / 0.25 h
View Scheme
参考文献
Wozniak, M.; Plas, H. C. van der; Tomula, M.; Veldhuizen, A. van
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, p. 511 - 513
反应条件
1: 60 percent / phosphoryl chloride / 15 h / Heating
2: 74 percent / ammonia / ethanol / 4 h / 110 °C
View Scheme
参考文献
Wozniak, M.; Plas, H. C. van der; Tomula, M.; Veldhuizen, A. van
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, p. 511 - 513
