3,4,5-三甲氧基苯酚合成路线 (共 94 条)
反应条件
1: K2CO3 / acetone / 10 h / Heating 2: 50percent KOH / ethanol / 120 h / Heating View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 26, # 7 p. 2075 - 2078
反应条件
1: benzene; PCl5 / man leitet dann Ammoniak ein 2: hypochlorite; sodium hydroxide / unter Eiszusatz 3: Diazotization.Kochen der Loesung mit Schwefelsaeure View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 340, p. 230
反应条件
potassium hydroxide in ethanol 120 h; Heating;
参考文献
Phytochemistry (Elsevier), , vol. 26, # 7 p. 2075 - 2078
反应条件
potassium hydroxide in ethanol Heating;
参考文献
Bulletin de la Societe Chimique de France, , p. 3617 - 3624
反应条件
1.1: magnesium / diethyl ether / Heating 1.2: diethyl ether / Heating 2.1: BF3*Et2O; NaBO3*4H2O / tetrahydrofuran / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 13, # 6 p. 1674 - 1691
反应条件
1: AcOOH, HClO4, Ac2O / acetic acid 2: KOH / aq. ethanol / Heating View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 3617 - 3624
反应条件
1.1: ammonia / acetone / 1 h / 0 - 20 °C 2.1: NaClO; sodium hydroxide / water / 20 - 100 °C 3.1: sulfuric acid; sodium nitrite / water / 10 - 15 °C 3.2: 2 h / 100 °C View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 45, # 4 p. 321 - 324
反应条件
tetraethylammonium bromide in water; N,N-dimethyl-formamide electrolysis;
参考文献
Akbulut, Ural; Toppare, Levent; Utley, James H. P.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 391 - 394
反应条件
potassium carbonate in acetone 3 h; Heating;
参考文献
Acta chemica Scandinavica (Copenhagen, Denmark : 1989), , vol. 50, # 6 p. 558 - 560
反应条件
potassium hydroxide; potassium carbonate 1.) Me2CO, reflux, 6 h, 2.) MeOH, reflux; Multistep reaction;
参考文献
Phytochemistry, , vol. 44, # 5 p. 943 - 947