3,4,5-三甲氧基苯酚合成路线 （共 94 条）
反应条件
1: With anhydrous butyl ether; bis[3,5-bis(trifluoromethyl)diphenyl] diselenide in 2,2,2-trifluoroethanol T=20°C; Baeyer-Villiger oxidation; 0.25 h; 2: With potassium hydroxide in methanol 2 h; Further stages.;
参考文献
Ten Brink; Vis; Arends; Sheldon
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2429 - 2433
反应条件
sodium perborate; boron trifluoride diethyl etherate in tetrahydrofuran T=0°C; 1.5 h;
参考文献
Kabalka; Reddy; Narayana
Tetrahedron Letters, 1993 , vol. 34, # 48 p. 7667 - 7668
反应条件
potassium hydroxide in methanol T=0 - 20°C;
参考文献
Narsaiah, A. Venkat; Nagaiah
Synthesis, 2010 , # 16 art. no. Z07610SS, p. 2705 - 2707
反应条件
1: With sulfuric acid; sodium nitrite in water T=10 - 15°C; 2: With sulfuric acid; copper(II) sulfate T=100°C; 2 h;
参考文献
Qin, Qi-Xue; Yang, Jian; Chen, Duo-Zhi; Yang, Bo; Zhang, Ji
Organic Preparations and Procedures International, 2013 , vol. 45, # 4 p. 321 - 324
反应条件
potassium hydroxide in methanol; water T=180°C;
参考文献
Journal of Organic Chemistry, , vol. 26, p. 2449 - 2453
反应条件
anhydrous butyl ether; bis[3,5-bis(trifluoromethyl)diphenyl] diselenide in 2,2,2-trifluoroethanol T=20°C; Baeyer-Villiger oxidation; 0.25 h;
参考文献
Journal of Organic Chemistry, , vol. 66, # 7 p. 2429 - 2433
反应条件
1: sodium dithionite 2: 120 mg / K2CO3 / acetone / 3 h / Heating View Scheme
参考文献
Acta chemica Scandinavica (Copenhagen, Denmark : 1989), , vol. 50, # 6 p. 558 - 560
反应条件
methanol; ammonium hydrogen carbonate; magnesium; palladium on activated charcoal T=20°C; 24 h;
参考文献
Chemistry - A European Journal, , vol. 13, # 5 p. 1432 - 1441
反应条件
methanol; ammonia; magnesium; palladium on activated charcoal T=20°C; 1.5 h;
参考文献
Chemistry - A European Journal, , vol. 13, # 5 p. 1432 - 1441
