17beta-甲基-5alpha-雄甾烷-3alpha,17beta-二醇合成路线 （共 5 条）
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=65°C; 2 h;
参考文献
Chhikara, Bhupender S.; Chandra, Ramesh; Tandon, Vibha
Tetrahedron Letters, 2004 , vol. 45, # 41 p. 7585 - 7588
参考文献
Ruzicka; Meister; Prelog
Helvetica Chimica Acta, 1947 , vol. 30, p. 867,873
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=65°C; 24 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 52, # 8 p. 989 - 991
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=65°C; 24 h;
参考文献
Chhikara, Bhupender S.; Chandra, Ramesh; Tandon, Vibha
Tetrahedron Letters, 2004 , vol. 45, # 41 p. 7585 - 7588
反应条件
1: Jones reagent / acetone 2: 3.0 g / pyridinium tribromide / ethanol; CH2Cl2 / 3 h / 40 °C 3: 2.04 g / LiBr; Li2CO3 / dimethylformamide / 2 h / Heating View Scheme
参考文献
Gauthier, Julie; Poirier, Donald; Ayotte, Christiane
Steroids, 2012 , vol. 77, # 6 p. 635 - 643
