N-2-丙烯-1-基-1H-吡咯并[2,3-B]吡啶-4-胺合成路线 （共 4 条）
反应条件
methanesulfonic acid; palladium on activated charcoal in ethanol T=105°C; 72 h;
参考文献
Thibault, Carl; L'Heureux, Alexandre; Bhide, Rajeev S.; Ruel, Rejean
Organic Letters, 2003 , vol. 5, # 26 p. 5023 - 5025
反应条件
1: 13.15 g / methanesulfonic acid / Pd/C / ethanol / 72 h / 105 °C 2: tetrafluoroboric acid; sodium nitrite / H2O / 22 h / 0 - 20 °C View Scheme
参考文献
Thibault, Carl; L'Heureux, Alexandre; Bhide, Rajeev S.; Ruel, Rejean
Organic Letters, 2003 , vol. 5, # 26 p. 5023 - 5025
反应条件
1: 13.15 g / methanesulfonic acid / Pd/C / ethanol / 72 h / 105 °C 2: 44 percent / tetrafluoroboric acid; sodium nitrite / H2O / 22 h / 0 - 20 °C View Scheme
参考文献
Thibault, Carl; L'Heureux, Alexandre; Bhide, Rajeev S.; Ruel, Rejean
Organic Letters, 2003 , vol. 5, # 26 p. 5023 - 5025
反应条件
palladium diacetate; sodium t-butanolate; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane
T=100°C; 16 h;
参考文献
Thibault, Carl; L'Heureux, Alexandre; Bhide, Rajeev S.; Ruel, Rejean
Organic Letters, 2003 , vol. 5, # 26 p. 5023 - 5025
