反应条件
1.1: 32 percent / SnCl2; AcOH; aq. HCl / 1 h / 20 °C 2.1: 84 percent / pyridine / CH2Cl2 / 12 h / 50 °C 3.1: lithium 4,4'-di-tert-butylbiphenylide / tetrahydrofuran / -100 - -41 °C 3.2: 51 percent / BrCF2CF2Br / tetrahydrofuran / -41 - 20 °C View Scheme
参考文献
Yamashita, Makoto; Yamamoto, Yohsuke; Akiba, Kin-Ya; Hashizume, Daisuke; Iwasaki, Fujiko; Takagi, Nozomi; Nagase, Shigeru
Journal of the American Chemical Society, 2005 , vol. 127, # 12 p. 4354 - 4371
