2,2,3,3,3-五氟三氟甲烷磺酸丙酯合成路线 （共 6 条）
反应条件
in N,N-dimethyl-formamide
参考文献
Journal of Organic Chemistry, , vol. 30, p. 4322 - 4324
参考文献
J. URIACH and CIA. S.A.
Patent: WO2004/9528 A1, 2004 ;
Location in patent: Page 29 ;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
参考文献
Hansen,R.L.
Journal of Organic Chemistry, 1965 , vol. 30, p. 4322 - 4324
参考文献
Minnesota Mining & Manufg. Co.
Patent: FR1470669 , 1967 ;
C.A., 1967 , vol. 67, p. 63788
反应条件
1: 2,4-dihydroxy-benzoic acid With sodium hydride in DMF (N,N-dimethyl-formamide)
T=20°C; 0.5 h;
2: With boric acid trimethyl ester in DMF (N,N-dimethyl-formamide)
T=20°C; 1 h;
3: 2,2,3,3,3-pentafluoropropyl trifluoromethanesulfonate in DMF (N,N-dimethyl-formamide)
T=100°C;
参考文献
J. URIACH and CIA. S.A.
Patent: WO2004/9528 A1, 2004 ;
Location in patent: Page 29 ;
