1-(4-甲氧基苄基)乙胺合成路线 （共 17 条）
反应条件
formic acid in water 5 h; Heating;
参考文献
Kmonicek, Vojtech; Vejdelek, Zdenek; Holubek, Jiri; Valchar, Martin; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 6 p. 1721 - 1733
反应条件
Candida antartica lipase B; triethylamine in n-heptane T=50°C; 25 h; Inert atmosphereEnzymatic reaction; optical yield given as percent ee;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 23 p. 8171 - 8177
反应条件
1: Candida antarctica lipase B 2: 3M aq. KOH / Heating View Scheme
参考文献
Munoz, Lourdes; Rodriguez, Anna M.; Rosell, Gloria; Bosch, M. Pilar; Guerrero, Angel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8171 - 8177
反应条件
Candida antartica lipase B; triethylamine T=35°C; Inert atmosphereEnzymatic reaction; optical yield given as percent ee;
参考文献
Munoz, Lourdes; Rodriguez, Anna M.; Rosell, Gloria; Bosch, M. Pilar; Guerrero, Angel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8171 - 8177
反应条件
hydrogen bromide in water 3 h; Reflux;
参考文献
Munoz, Lourdes; Rodriguez, Anna M.; Rosell, Gloria; Bosch, M. Pilar; Guerrero, Angel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8171 - 8177
反应条件
ethanol; sodium acetate; nickel Hydrogenation;
参考文献
Woodruff; Lambooy; Burt
Journal of the American Chemical Society, 1940 , vol. 62, p. 922
反应条件
1: hydrogen bromide / water / 3 h / Reflux 2: Candida antartica lipase B; triethylamine / 96 h / 35 °C / Inert atmosphere; Enzymatic reaction View Scheme
参考文献
Munoz, Lourdes; Rodriguez, Anna M.; Rosell, Gloria; Bosch, M. Pilar; Guerrero, Angel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8171 - 8177
参考文献
van Dijk,J. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1965 , vol. 84, p. 521 - 539
反应条件
1: 100 percent / 6 h / 120 - 130 °C / in autoclave
2: 98 percent / lithium aluminium hydride / diethyl ether / 2 h / Heating
View Scheme
参考文献
Woodruff; Lambooy; Burt
Journal of the American Chemical Society, 1940 , vol. 62, p. 922
Full Text View citing articles Show Details
Sawizkii; Machnenko
Zhurnal Obshchei Khimii, 1940 , vol. 10, p. 1819,1822
Chem. Zentralbl., 1942 , vol. 113, # I p. 2764
Full Text Show Details
Alles
Patent: US2015578 , 1933 ;
参考文献
Knoll A.G.
Patent: DE675361 , 1936 ;
DRP/DRBP Org.Chem.
