in carbon disulfide
react. of asoln. of the elements in CS2 at 0 °C; discoloration of the soln.;; sucking off the solvent; pptn. of crystals; removal of of CS2 in vac.;;
参考文献
Baudler, M.; Fricke, G.; Fichtner, K.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1964 , vol. 327, p. 124 - 127
in neat (no solvent)
byproducts: KCl; on-line process; SPCl3 degassed in vac. line using liq. N2; SPCl3 vapor passed via vac. line over solid KI at 440°C (slow flow, 0.2 torr)into IR cell; detd. by IR spectra;
参考文献
Zidan, Mohammed D.; Allaf, Abdul W.
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2002 , vol. 58, # 8 p. 1577 - 1582
