(2-三甲基硅基乙基)三苯基碘化磷合成路线 (共 5 条)
参考文献
Journal of Organometallic Chemistry, , vol. 181, p. 293 - 304
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) 3 h, 0 deg C; 2.) overnight, RT;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 107, # 4 p. 313 - 324
反应条件
1: n-BuLi / hexane; tetrahydrofuran / 1.5 h / 0 - 20 °C 2: hexane; tetrahydrofuran / 1.5 h / 0 - 20 °C View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 181, # 10 p. 2283 - 2295
反应条件
(i) MeLi, (ii) /BRN= 471223/; Multistep reaction;
参考文献
Seyferth,D. et al.
Journal of Organometallic Chemistry, 1979 , vol. 181, p. 293 - 304
反应条件
methyllithium
1.) Et2O, RT, 1 h, 2.) Et2O, RT, 4 h; Yield given. Multistep reaction;
参考文献
Seyferth, Dietmar; Wursthorn, Karl R.; Lim, Thomas F. O.; Sepelak, Dennis J.
Journal of Organometallic Chemistry, 1981 , vol. 205, # 3 p. 301 - 310