2-(4-甲氧基苯基)环氧乙烷合成路线 （共 33 条）
反应条件
sodium hypochlorite; potassium bromide in phosphate buffer; acetonitrile
T=40°C; pH=10.4; 0.333333 h;
参考文献
Klawonn, Markus; Bhor, Santosh; Mehltretter, Gerald; Doebler, Christian; Fischer, Christine; Beller, Matthias
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 3 p. 389 - 392
反应条件
2,6-dichloropyridine-N-oxide; Ru(IV)(TDCPP)Cl2 in chloroform-d1
T=25°C; 0.25 h;
参考文献
Hu, Wen-Xiang; Li, Pei-Rong; Jiang, Gaoxi; Che, Chi-Ming; Chen, Jian
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3190 - 3194
反应条件
1: With orthoacetic acid trimethyl ester; chloro-trimethyl-silane in dichloromethane
T=0°C; 1 h; Inert atmosphere;
2: With potassium carbonate in methanol
1.6 h; Inert atmosphere;
参考文献
Karad, Somnath Narayan; Bhunia, Sabyasachi; Liu, Rai-Shung
Angewandte Chemie - International Edition, 2012 , vol. 51, # 35 p. 8722 - 8726
参考文献
Sato; Kosasayama; Uchimaru
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 10 p. 2885 - 2892
反应条件
1: potassium carbonate / dioxane; H2O / Heating
2: 3-chloroperbenzoic acid; NaHCO3 / CH2Cl2; H2O / 2.5 h / 20 °C
View Scheme
参考文献
Bernasconi, Silvana; Orsini, Fulvia; Sello, Guido; Di Gennaro, Patrizia
Tetrahedron Asymmetry, 2004 , vol. 15, # 10 p. 1603 - 1606
反应条件
1: 96.2 percent / NaBH4 / methanol / 2 °C
2: 49.9 percent / 4 N NaOH
View Scheme
参考文献
Sato; Kosasayama; Uchimaru
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 10 p. 2885 - 2892
反应条件
water; zeolite NaY
2 h; in dark; Yield givenYields of byproduct given;
参考文献
Matsubara, Chie; Kojima, Masanobu
Tetrahedron Letters, 1999 , vol. 40, # 17 p. 3439 - 3442
反应条件
oxygen; zeolite NaY
2 h; Irradiation; Yield givenYields of byproduct given;
参考文献
Matsubara, Chie; Kojima, Masanobu
Tetrahedron Letters, 1999 , vol. 40, # 17 p. 3439 - 3442
反应条件
potassium hydroxide
1) CH3CN, H2O, 52 deg C, 15 min 2) CH3CN, 60 min; Yield given. Multistep reaction;
参考文献
Borredon, E.; Clavellinas, F.; Delmas, M.; Gaset, A.; Sinisterra, J. V.
Journal of Organic Chemistry, 1990 , vol. 55, # 2 p. 501 - 504
反应条件
in tetrahydrofuran; dimethyl sulfoxide
1.) 0-5 deg C, 15 min., 2.) r.t., 90 min; Yield given;
参考文献
Alvarez; Granados; Lavilla; Salas
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 3 p. 745 - 750
