2-(4-甲氧基苯基)环氧乙烷合成路线 (共 33 条)
反应条件
activated silica
24 h; Inert atmosphere; regioselective reaction;
参考文献
Saxena, Anil K.; Sharma, Sugandha; Pandey, Atindra K.; Shukla, Praveen K.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 21 p. 6476 - 6481
反应条件
sodium hydride in dimethyl sulfoxide
0.5 h; Ambient temperature;
参考文献
Kumar, Ashok; Singh, Rajeshwar; Mandal, Arun K
Synthetic Communications, 1982 , vol. 12, # 8 p. 613 - 620
反应条件
1H-imidazole; TPPMnOAc; tetrabutylammonium hydrogen monopersulfate in dichloromethane
T=20°C; 0.5 h;
参考文献
Aghabali, Amineh; Safari, Nasser
Journal of Porphyrins and Phthalocyanines, 2010 , vol. 14, # 4 p. 335 - 342
反应条件
1H-imidazole; C42H27FeN8O2; tetrabutylammonium (meta)periodate in dichloromethane
T=20°C; 4 h;
参考文献
Zakavi, Saeed; Mokary Yazdeli, Tahereh
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 367, p. 108 - 115
反应条件
caesium carbonate in tetrahydrofuran
T=80°C; 12 h;
参考文献
Forbes, David C.; Bettigeri, Sampada V.; Patrawala, Samit A.; Pischek, Susanna C.; Standen, Michael C.
Tetrahedron, 2009 , vol. 65, # 1 p. 70 - 76
反应条件
sodium hydride in dimethyl sulfoxide
参考文献
Guy; Doussot; Ferroud; Garreau; Godefroy-Falguieres
Synthesis, 1992 , # 9 p. 821 - 822
反应条件
sodium hydroxide in dichloromethane; water
T=50°C; Corey-Chaykovsky reaction; Phase-transfer catalyst;
参考文献
Afon'kin; Kostrikin; Shumeiko; Popov
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 12 p. 1776 - 1779
反应条件
cesium fluoride in dimethyl sulfoxide
15 h; Ambient temperature;
参考文献
Hioki; Tani; Sato
Synthesis, 1995 , # 6 p. 649 - 650
反应条件
1: With tetramethylene sulfide; N,N,N',N'-tetra-methylnaphthalene-1,8-diamine in dichloromethane
T=20°C; 0.416667 h; Inert atmosphere;
2: With 1-tert-butyl-2,2,4,4,4-pentakis(dimethylamino)-25,45-catenodi(phosphazene) in tetrahydrofuran; dichloromethane
T=20°C; Inert atmosphere;
参考文献
Piccinini, Alessandro; Kavanagh, Sarah A.; Connon, Paul B.; Connon, Stephen J.
Organic Letters, 2010 , vol. 12, # 3 p. 608 - 611
反应条件
sodium methylate in acetonitrile
Corey-Chaykovsky reaction; 2.5 h;
参考文献
Afon'kin; Kostrikin; Shumeiko; Popov
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 12 p. 1776 - 1779