4-甲氧基-5-硝基-1,1-联苯-2-醇合成路线 （共 15 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in 1,4-dioxane; water
T=100°C; 20 h; Inert atmosphere;
参考文献
Zhao, Jiaji; Wang, Yong; He, Yimiao; Liu, Lanying; Zhu, Qiang
Organic Letters, 2012 , vol. 14, # 4 p. 1078 - 1081
反应条件
sodium hydroxide in ethanol
20 h;
参考文献
Werbel; Cook; Elslager; Hung; Johnson; Kesten; McNamara; Ortwine; Worth
Journal of Medicinal Chemistry, 1986 , vol. 29, # 6 p. 924 - 939
反应条件
copper
T=180°C; 24 h;
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
反应条件
T=180°C; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
反应条件
T=180°C; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
反应条件
1: 55 percent / tetrahydrothiophene 1,1-dioxide / 2 h / 80 °C
2: 5 h / 180 °C
View Scheme
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
反应条件
pyridine hydrochloride
T=150°C;
参考文献
Astles, Peter C.; Brown, Thomas J.; Cox, Paul; Halley, Frank; Lockey, Peter M.; McCarthy, Clive; McLay, Iain M.; Majid, Tahir N.; Morley, Andrew D.; Porter, Barry; Ratcliffe, Andrew J.; Walsh, Roger J.A.
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 7 p. 907 - 912
反应条件
1: Pd(PPh3)4 / toluene / Heating
2: pyridine*HCl / 150 °C
View Scheme
参考文献
Astles, Peter C.; Brown, Thomas J.; Cox, Paul; Halley, Frank; Lockey, Peter M.; McCarthy, Clive; McLay, Iain M.; Majid, Tahir N.; Morley, Andrew D.; Porter, Barry; Ratcliffe, Andrew J.; Walsh, Roger J.A.
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 7 p. 907 - 912
反应条件
1: Pd(PPh3)4 / toluene / Heating
2: pyridine*HCl / 150 °C
View Scheme
参考文献
Astles, Peter C.; Brown, Thomas J.; Cox, Paul; Halley, Frank; Lockey, Peter M.; McCarthy, Clive; McLay, Iain M.; Majid, Tahir N.; Morley, Andrew D.; Porter, Barry; Ratcliffe, Andrew J.; Walsh, Roger J.A.
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 7 p. 907 - 912
反应条件
T=180°C; 5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
