反应条件
in methanol
soln. refluxed (several h); excess of thallium carbonate sepd., solvent removed, solid washed with Et2O, recrystd. from ethanol repeatedly, dried (vac., room temp.); detn. of purity (99.86 mol percent) by DSC;
参考文献
Roux, M. V.; Turrion, C.; Fernandez-Martin, F.; Fuente, F. L. Lopez de la; Cheda, J. A. R.
Thermochimica Acta, 1989 , vol. 139, p. 139 - 148
