乙酰乙酰-2,5-二甲氧基苯胺合成路线 (共 10 条)
参考文献
Maiti, Arup; Reddy, P. V. Narasimha; Sturdy, Megan; Marler, Laura; Pegan, Scott D.; Mesecar, Andrew D.; Pezzuto, John M.; Cushman, Mark
Journal of Medicinal Chemistry, 2009 , vol. 52, # 7 p. 1873 - 1884
反应条件
in xylene T=120°C; 0.5 h;
参考文献
Avendano; De la Cuesta; Gesto
Synthesis, 1991 , # 9 p. 727 - 730
反应条件
silver trifluoroacetate in ethylene glycol dimethyl ether Ambient temperature;
参考文献
Lopez-Alvarado, Pilar; Avendano, Carmen; Menendez, J. Carlos
Synthesis, 1998 , # 2 p. 186 - 194
参考文献
Journal of the American Chemical Society, , vol. 68, p. 644,645
反应条件
in toluene 24 h; RefluxInert atmosphere;
参考文献
Wang, Min; Gao, Mingzhang; Miller, Kathy D.; Sledge, George W.; Hutchins, Gary D.; Zheng, Qi-Huang
Steroids, 2010 , vol. 75, # 12 p. 967 - 973
反应条件
1: concentrated sulfuric acid
2: phosphoryl chloride
3: sodium methylate; methanol
View Scheme
参考文献
Kaslow; Sommer
Journal of the American Chemical Society, 1946 , vol. 68, p. 644,645
反应条件
toluene-4-sulfonic acid in benzene
24 h; Heating;
参考文献
Pierce, James Benjamin; Ariyan, Zaven S.; Ovenden, Gaye Stuart
Journal of Medicinal Chemistry, 1982 , vol. 25, # 2 p. 131 - 136
反应条件
1: concentrated sulfuric acid
2: phosphoryl chloride
View Scheme
参考文献
Kaslow; Sommer
Journal of the American Chemical Society, 1946 , vol. 68, p. 644,645
反应条件
1: concentrated sulfuric acid
2: phosphoryl chloride
3: acetic acid; palladium; sodium acetate / 70 °C / Hydrogenation
View Scheme
参考文献
Kaslow; Sommer
Journal of the American Chemical Society, 1946 , vol. 68, p. 644,645