[(P{(C6H11)3})2Pd(Cl)2]; hydrogen; triethylamine in benzene T=155°C; P=53200 Torr; 6 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 119, # 27 p. 6448 - 6449
p-toluenesulfonic acid in tetrahydrofuran Ni complex transferred to NMR tube and capped with a rubber septum, added alkyne via syringe at room temp. then added TsOH; yields calcd. by GC;
参考文献
Journal of the American Chemical Society, , vol. 103, # 11 p. 3002 - 3011