1H-吡唑并[3,4-b]吡啶-3-重氮四氟硼酸盐(1-)合成路线 （共 4 条）
反应条件
1: hypophosphorous acid / water / 20 °C 2: iodine; potassium hydroxide / N,N-dimethyl-formamide / 20 °C View Scheme
参考文献
Ye, Qing; Shen, Yanhong; Zhou, Yubo; Lv, Dan; Gao, Jianrong; Li, Jia; Hu, Yongzhou
European Journal of Medicinal Chemistry, 2013 , vol. 68, p. 361 - 371
反应条件
hypophosphorous acid in water T=20°C;
参考文献
Ye, Qing; Shen, Yanhong; Zhou, Yubo; Lv, Dan; Gao, Jianrong; Li, Jia; Hu, Yongzhou
European Journal of Medicinal Chemistry, 2013 , vol. 68, p. 361 - 371
反应条件
tetrafluoroboric acid; CHMe2CH2CH2NO2 in methanol
T=0 - 5°C;
参考文献
Ye, Qing; Shen, Yanhong; Zhou, Yubo; Lv, Dan; Gao, Jianrong; Li, Jia; Hu, Yongzhou
European Journal of Medicinal Chemistry, 2013 , vol. 68, p. 361 - 371
反应条件
1: hydrazine hydrate / ethanol / |Reflux
2: CHMe2CH2CH2NO2; tetrafluoroboric acid / methanol / 0 - 5 °C
View Scheme
参考文献
Ye, Qing; Shen, Yanhong; Zhou, Yubo; Lv, Dan; Gao, Jianrong; Li, Jia; Hu, Yongzhou
European Journal of Medicinal Chemistry, 2013 , vol. 68, p. 361 - 371
