4,6-O-苄烯-D-己烯糖合成路线 （共 18 条）
反应条件
1: 89 percent / 4-dimethylaminopyridine, pyridine / 0.25 h / 0 °C 2: 92 percent / NaIO4, RuCl3*3H2O / CCl4; acetonitrile; H2O / 0.25 h / Ambient temperature 3: 86 percent / lithium naphthalene / tetrahydrofuran / -78 °C View Scheme
参考文献
Carbohydrate Research, , vol. 244, # 2 p. 247 - 258
反应条件
1: 92 percent / NaIO4, RuCl3*3H2O / CCl4; acetonitrile; H2O / 0.25 h / Ambient temperature 2: 86 percent / lithium naphthalene / tetrahydrofuran / -78 °C View Scheme
参考文献
Carbohydrate Research, , vol. 244, # 2 p. 247 - 258
反应条件
sodium tetrahydroborate; cerium(III) chloride in ethanol 0.333333 h; Inert atmosphereCooling with ice; optical yield given as percent de;
参考文献
Carbohydrate Research, , vol. 343, # 16 p. 2740 - 2743
反应条件
sodium azide; sodium 1.) HMPA, 90 deg C, 400 h, 2.) MeOH, RT, 2 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Australian Journal of Chemistry, , vol. 33, # 11 p. 2499 - 2508
反应条件
methanol; sodium; triphenylphosphine; diethylazodicarboxylate 1.) THF, RT, 1 h; 2.) RT, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 468 - 472
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 468 - 472
反应条件
perchloric acid T=20°C; 0.333333 h;
参考文献
Agnihotri, Geetanjali; Misra, Anup Kumar
Tetrahedron Letters, 2006 , vol. 47, # 22 p. 3653 - 3658
反应条件
perchloric acid in acetonitrile T=20°C; 0.25 h;
参考文献
Agnihotri, Geetanjali; Misra, Anup Kumar
Tetrahedron Letters, 2006 , vol. 47, # 22 p. 3653 - 3658
