反应条件
1: 1.) NaH, (iPr)2NH, 2.) n-BuLi / 1.) THF, 0 deg C and reflux, 15 min, 2.) THF, HMPA, 0 deg C, 15 min and 35 deg C 30 min, 3.) THF, HMPA, 0 deg C and 3 h, 25 deg C
2: 91 percent / LiAlH4 / diethyl ether / 10 h / 0 °C
3: Et3N / CH2Cl2 / 1 h / 0 °C
4: NaI / acetone / 12 h / Heating
View Scheme
参考文献
Curran, Dennis P.; Yu, Hosung; Liu, Hongtao
Tetrahedron, 1994 , vol. 50, # 25 p. 7343 - 7366
