1,1'-(1H-吡咯-2,4-二基)二乙酮合成路线 (共 11 条)
反应条件
trifluoroacetic anhydride in benzene
T=20°C; 336000 h;
参考文献
Hou, Shifa; Ding, Mengxian; Gao, Lianxun
Macromolecules, 2003 , vol. 36, # 11 p. 3826 - 3832
反应条件
tetrafluoroboric acid; mercury(II) oxide in dimethyl sulfoxide
0.5 h; Ambient temperature;
参考文献
Cadamuro, Silvano; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Gatti, Antonella; Piscopo, Laura
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 2 p. 273 - 284
反应条件
tetrafluoroboric acid; mercury(II) oxide in dimethyl sulfoxide
0.5 h; Ambient temperature;
参考文献
Cadamuro, Silvano; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Gatti, Antonella; Piscopo, Laura
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 2 p. 273 - 284
反应条件
aluminium trichloride in dichloromethane
0.5 h; Ambient temperature;
参考文献
Cadamuro, Silvano; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Gatti, Antonella; Piscopo, Laura
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 2 p. 273 - 284
反应条件
tetrafluoroboric acid; mercury(II) oxide in dimethyl sulfoxide
2 h; Ambient temperature;
参考文献
Cadamuro, Silvano; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Gatti, Antonella; Piscopo, Laura
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 2 p. 273 - 284
反应条件
aluminium trichloride in dichloromethane
3 h; Heating;
参考文献
Cadamuro, Silvano; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Gatti, Antonella; Piscopo, Laura
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 2 p. 273 - 284
反应条件
1: 94.4 percent / aq. NaOH / methanol / 4 h / Heating
2: 45.1 percent / trifluoroacetic anhydride / benzene / 336000 h / 20 °C
View Scheme
参考文献
Hou, Shifa; Ding, Mengxian; Gao, Lianxun
Macromolecules, 2003 , vol. 36, # 11 p. 3826 - 3832
反应条件
amberlyst-15
T=45°C; 3 h;
参考文献
Das, Biswanath; Pal, Rammohan; Banerjee, Joydeep; Mahender; Holla, Harish; Venkateswarlu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 1 p. 198 - 200
反应条件
1: 100 percent / aq. 17percent NaOH / dioxane / 15 h / Ambient temperature
2: 92 percent / anhydrous AlCl3 / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
参考文献
Cadamuro, Silvano; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Gatti, Antonella; Piscopo, Laura
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 2 p. 273 - 284
反应条件
1: 100 percent / HBF4-diethyl ether complex / ethanol / 1 h / Ambient temperature
2: 91 percent / HgO, 35percent aq. HBF4 / dimethylsulfoxide / 0.5 h / Ambient temperature
View Scheme
参考文献
Cadamuro, Silvano; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Gatti, Antonella; Piscopo, Laura
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 2 p. 273 - 284