反应条件
1.1: bis-triphenylphosphine-palladium(II) chloride; diethylamine; copper(l) chloride / 0 - 20 °C / Inert atmosphere
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: indium trifluoromethanesulfonate; butan-1-ol / dichloromethane / 3 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Miura, Katsukiyo; Yamamoto, Kiyomi; Yamanobe, Aya; Ito, Keisuke; Kinoshita, Hidenori; Ichikawa, Junji; Hosomi, Akira
Chemistry Letters, 2010 , vol. 39, # 7 p. 766 - 767