5-氯-2-甲氧基苯乙酮合成路线 （共 20 条）
反应条件
potassium carbonate in DMF (N,N-dimethyl-formamide) T=20°C;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/19184 A1, 2005 ;
Location in patent: Page/Page column 74 ;
WO 2005/019184 A1
反应条件
potassium carbonate; methyl iodide in acetonitrile T=85°C; 18 h;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/19184 A1, 2005 ;
Location in patent: Page/Page column 43-44 ;
WO 2005/019184 A1
反应条件
bis[2-(N,N-dimethylamino)ethyl] ether in tetrahydrofuran Grignard reaction; cooling;
参考文献
Wang, Xiao-Jun; Zhang, Li; Sun, Xiufeng; Xu, Yibo; Krishnamurthy, Dhileepkumar; Senanayake, Chris H.
Organic Letters, 2005 , vol. 7, # 25 p. 5593 - 5595
反应条件
1: in tetrahydrofuran 6 h; Reflux; 2: With hydrogenchloride in water T=75°C; 20 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 619 - 622
反应条件
1: Lewis acid / nitrobenzene / Heating View Scheme
参考文献
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, , vol. 37, # 3 p. 199 - 204
反应条件
aluminium trichloride
参考文献
Yuldashev, Kh. Yu.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1610 - 1612
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 9 p. 1893 - 1895
反应条件
iron(III) chloride 4 h; heating;
参考文献
Yuldashev, Kh. Yu.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1610 - 1612
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 9 p. 1893 - 1895
参考文献
Journal of the Indian Chemical Society, , vol. 26, p. 366,367
反应条件
ethanol; sodium ethanolate
参考文献
Journal of the Indian Chemical Society, , vol. 17, p. 65,71
反应条件
carbon disulfide; aluminium trichloride zuletzt auf dem Wasserbad;
参考文献
Chemische Berichte, , vol. 57, p. 92
Justus Liebigs Annalen der Chemie, , vol. 446, p. 157 Anm. 2, 177
