3-(4-溴苯甲酰)丙酸合成路线 （共 54 条）
参考文献
Journal of the American Chemical Society, , vol. 39, p. 2414
参考文献
Collection of Czechoslovak Chemical Communications, vol. 1, p. 343
Chem. Zentralbl., , vol. 100, # II p. 998
反应条件
1: 98 percent / KOH; H2NNH2 / triethylene glycol / 2 h / 200 °C 2: 95 percent / polyphosphoric acid / 2 h / 90 °C 3: 99 percent / p-TsOH / benzene / 48 h / 105 °C View Scheme
参考文献
Sommer; Rheingold; Goshe; Bosnich
Journal of the American Chemical Society, 2001 , vol. 123, # 17 p. 3940 - 3952
反应条件
1: N2H4, aq. KOH View Scheme
参考文献
Tsuno,Y. et al.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, p. 3033 - 3042
反应条件
potassium hydroxide; hydrazine in 1,2-bis-(2-hydroxyethoxy)-ethane T=200°C; Wolff-Kishner reduction; 2 h;
参考文献
Sommer; Rheingold; Goshe; Bosnich
Journal of the American Chemical Society, 2001 , vol. 123, # 17 p. 3940 - 3952
反应条件
hydrogenchloride; amalgamated zinc; toluene weiteres Reagens: Essigsaeure;
参考文献
Fieser; Seligman
Journal of the American Chemical Society, 1938 , vol. 60, p. 170,174
参考文献
Fieser; Seligman
Journal of the American Chemical Society, 1938 , vol. 60, p. 170,174
反应条件
1: 82 percent / KOH; hydrazine monohydrate / triethylene glycol / 90 - 200 °C 2: 75 percent / polyphosphoric acid / 1 h / 80 °C View Scheme
参考文献
Sommer; Rheingold; Goshe; Bosnich
Journal of the American Chemical Society, 2001 , vol. 123, # 17 p. 3940 - 3952
反应条件
hydrazine in ethanol 2 h; Heating / reflux;
参考文献
ABBOTT LABORATORIES
Patent: WO2006/65233 A1, 2006 ;
Location in patent: Page/Page column 75 ;
参考文献
Abbott Laboratories
Patent: US2005/245531 A1, 2005 ;
US 20050245531 A1
