2-氨基-1,3-苯二酚盐酸盐合成路线 （共 7 条）
反应条件
iron; ammonium chloride in ethanol; water 0.25 h; Heating;
参考文献
Mobinikhaledi, Akbar; Foroughifar, Naser; Jirandehi, Hasan Fathinejad
Monatshefte fur Chemie, 2007 , vol. 138, # 8 p. 755 - 757
反应条件
hydrogenchloride; tin
参考文献
Chemische Berichte, , vol. 39, p. 326
反应条件
1: 79 percent / triethylamine / dimethylformamide / 15 h / Ambient temperature 2: 2.) manganese dioxide / 1.) toluene, RT, 17 h, 2.) ethanol, RT, 30 min 3: 71 percent / manganese dioxide / dimethylsulfoxide / 44 h / Ambient temperature View Scheme
参考文献
Yamane; Hashizume; Yamashita; Konishi; Hosoe; Hidaka; Watanabe; Kawaharada; Yamamoto; Kuze
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 1 p. 148 - 155
反应条件
1: 79 percent / triethylamine / dimethylformamide / 15 h / Ambient temperature 2: 2.) manganese dioxide / 1.) toluene, RT, 17 h, 2.) ethanol, RT, 30 min 3: 72 percent / manganese dioxide / dimethylsulfoxide / 24 h / Ambient temperature View Scheme
参考文献
Yamane; Hashizume; Yamashita; Konishi; Hosoe; Hidaka; Watanabe; Kawaharada; Yamamoto; Kuze
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 1 p. 148 - 155
反应条件
1: 79 percent / triethylamine / dimethylformamide / 15 h / Ambient temperature 2: 2.) manganese dioxide / 1.) toluene, RT, 17 h, 2.) ethanol, RT, 30 min 3: 70 percent / manganese dioxide / dimethylsulfoxide / 25 h / Ambient temperature View Scheme
参考文献
Yamane; Hashizume; Yamashita; Konishi; Hosoe; Hidaka; Watanabe; Kawaharada; Yamamoto; Kuze
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 1 p. 148 - 155
反应条件
3 h; Heating / reflux;
参考文献
Darwin Discovery, Ltd.
Patent: US6353010 B1, 2002 ;
Location in patent: Page column 14 ;
反应条件
1: 79 percent / triethylamine / dimethylformamide / 15 h / Ambient temperature 2: 2.) manganese dioxide / 1.) toluene, RT, 17 h, 2.) ethanol, RT, 30 min 3: 38 percent / manganese dioxide / dimethylsulfoxide / 42 h / Ambient temperature View Scheme
参考文献
Yamane; Hashizume; Yamashita; Konishi; Hosoe; Hidaka; Watanabe; Kawaharada; Yamamoto; Kuze
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 1 p. 148 - 155
