反应条件
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.08 h / 0 °C / |Inert atmosphere
1.2: 2 h / 0 - 20 °C / |Inert atmosphere
2.1: [2,2']bipyridinyl; potassium tert-butylate / 1,3,5-trimethyl-benzene / 24 h / 110 °C / |Inert atmosphere; |Schlenk technique; |Sealed tube
View Scheme
参考文献
De, Subhadip; Mishra, Sourabh; Kakde, Badrinath N.; Dey, Dhananjay; Bisai, Alakesh
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 7823 - 7844
