1,2,3-三甲氧基苯合成路线 （共 210 条）
反应条件
bromine in dichloromethane T=0 - 25°C;
参考文献
Wang, Jin-Liang; Li, Xiaopeng; Lu, Xiaocun; Hsieh, I-Fan; Cao, Yan; Moorefield, Charles N.; Wesdemiotis, Chrys; Cheng, Stephen Z. D.; Newkome, George R.
Journal of the American Chemical Society, 2011 , vol. 133, # 30 p. 11450 - 11453
反应条件
N-iodo-succinimide in various solvent(s) T=27°C; 0.25 h;
参考文献
Yadav; Reddy; Basak; Narsaiah
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 1 p. 77 - 82
反应条件
chlorine; acetic acid
参考文献
Jain, Subhash C.; Kumar, Ravindra; Gupta, Bhavna; Olsen, Carl E.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 10 p. 2200 - 2202
参考文献
Friedman; Ginsburg
Journal of Organic Chemistry, 1958 , vol. 23, p. 16
反应条件
carbon disulfide; aluminium trichloride
参考文献
Weizmann; Bergmann
Journal of the Chemical Society, 1936 , p. 567
反应条件
1: 1.) aluminium chloride, 2.) sodium dithionite, sodium hydroxide / 1.) 1,1,2,2-tetrachloroethane, room temperature, 16 h; steam-bath, 2 h, 2.) methanol, room temperature, 21 h, reflux, 24 h 2: 88 percent / hydrogen / palladium-carbon / acetic acid / 1.5 h / Ambient temperature 3: 59 percent / lithium aluminium hydride / diethyl ether 4: 62 percent / pyridine 5: 80 percent / lithium bromide / acetone / 24 h / Ambient temperature 6: magnesium (from magnesium chloride and potassium metal, 3-(4-methoxyphenyl)propanal / tetrahydrofuran 7: 74 percent / pyridinium chlorochromate / CH2Cl2 / 4.5 h View Scheme
参考文献
Henley-Smith, Peter; Whiting, Donald A.; Wood, Andrew F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 614 - 622
反应条件
NISacc T=20°C; Ionic liquidDarkness;
参考文献
Bailey, Lindsey; Handy, Scott T.
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2413 - 2414
反应条件
potassium peroxymonosulfate in acetonitrile-D3; water-d2; tert-butyl alcohol T=20°C; 5 h; Schlenk techniqueInert atmosphere;
参考文献
Collom; Anastas; Beach; Crabtree; Hazari; Sommer
Tetrahedron Letters, 2013 , vol. 54, # 19 p. 2344 - 2347
反应条件
dihydrogen peroxide; acetic acid; potassium hexacyanoferrate(III) T=20°C; 24 h;
参考文献
Chen, Wen-Hao; Wang, Rui; Shi, Yan-Ping
Journal of Natural Products, 2010 , vol. 73, # 8 p. 1398 - 1403
反应条件
dihydrogen peroxide in formic acid; water T=40°C; 2 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 5 p. 1652 - 1657
