1,2,3-三甲氧基苯合成路线 （共 210 条）
反应条件
methanol; ammonium hydrogen carbonate; magnesium; palladium on activated charcoal T=20°C; 24 h;
参考文献
Chemistry - A European Journal, , vol. 13, # 5 p. 1432 - 1441
反应条件
methanol; ammonia; magnesium; palladium on activated charcoal T=20°C; 1.5 h;
参考文献
Chemistry - A European Journal, , vol. 13, # 5 p. 1432 - 1441
反应条件
4-(N,N-dimethlyamino)pyridine T=110°C; 4 h;
参考文献
Barcelo, Gerard; Grenouillat, Denis; Senet, Jean-Pierre; Sennyey, Gerard
Tetrahedron, 1990 , vol. 46, # 6 p. 1839 - 1848
反应条件
1: 1) NaH / 1) THF 2) 3h, room temperature 2: 92 percent Chromat. / DMAP / 4 h / 110 °C View Scheme
参考文献
Tetrahedron, , vol. 46, # 6 p. 1839 - 1848
反应条件
1: 1.) Pb(OAc)4 / 1.) benzene, 60 deg C, 7 h, 2.) CHCl3-MeOH, 2 d, r.t. 2: 26 mg / K2CO3 / acetone View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 29, # 10 p. 2893 - 2898
反应条件
1: 180 mg / K2CO3 / acetone / 5 h / 50 °C 2: 1.) Pb(OAc)4 / 1.) benzene, 60 deg C, 7 h, 2.) CHCl3-MeOH, 2 d, r.t. 3: 26 mg / K2CO3 / acetone View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 29, # 10 p. 2893 - 2898
反应条件
potassium carbonate in acetone
参考文献
Ikeya, Yukinobu; Taguchi, Heihachiro; Yoshioka, Itiro
Chemical & Pharmaceutical Bulletin, 1981 , vol. 29, # 10 p. 2893 - 2898
反应条件
1: potassium tert-butylate / ethanol / 20 °C 2: oxygen; copper diacetate; silver carbonate / N,N-dimethyl-formamide / 18 h / 145 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 24 p. 9938 - 9941
反应条件
copper bronze 1.) 240 deg C, 0.5 h, 2.) from 240 deg C to 280 deg C, 0.5 h; Further byproducts given;
参考文献
Australian Journal of Chemistry, , vol. 34, # 4 p. 799 - 817
反应条件
1: With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=0°C; 2: With methanol in tetrahydrofuran Reactivity;
参考文献
Journal of Organic Chemistry, , vol. 74, # 7 p. 2760 - 2764
