2-[2-(2-AMINOETHOXY)ETHOXY]ETHANOL合成路线 （共 22 条）
反应条件
water; triphenylphosphine in tetrahydrofuran 4 h; Ambient temperature;
参考文献
Dykhuizen, Emily C.; Kiessling, Laura L.
Organic Letters, 2009 , vol. 11, # 1 p. 193 - 196
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=70°C; P=52505.3 Torr; Continuous-flow conditions;
参考文献
Howarth, Nicola M.; Ricci, Jennyfer
Tetrahedron, 2011 , vol. 67, # 49 p. 9588 - 9594
反应条件
hydrazine hydrate in ethanol 3 h; Reflux;
参考文献
Yerramreddy, Thirupathi Reddy; Milewski, Mikolaj; Penthala, Narsimha Reddy; Stinchcomb, Audra L.; Crooks, Peter A.
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 11 p. 3280 - 3283
反应条件
1: With potassium phtalimide in N,N-dimethyl-formamide T=100°C; 19 h; 2: With hydrazine hydrate in ethanol; water 3 h; Reflux;
参考文献
Isono, Takuya; Satoh, Toshifumi; Kakuchi, Toyoji
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 14 p. 3184 - 3192
反应条件
1: 65 percent / 50percent NaOH / H2O / 24 h / Heating 2: 88 percent / SOCl2 / 18 h / 80 °C 3: 98 percent / NaN3 4: 92 percent / H2 / Pd View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 9 p. 2672 - 2691
参考文献
Gartiser, Thierry; Selve, Claude; Mansuy, Laurence; Robert, Alain; Delpuech, Jean-Jacques
Journal of Chemical Research, Miniprint, 1984 , # 9 p. 2672 - 2691
反应条件
1: sodium azide / N,N-dimethyl-formamide / 20 °C 2: palladium on carbon; hydrogen / tetrahydrofuran View Scheme
参考文献
Inorganica Chimica Acta, , vol. 365, # 1 p. 38 - 48
反应条件
1: 88 percent / NaN3 / acetonitrile / 36 h / Heating 2: 100 percent / triphenylphosphine, H2O / tetrahydrofuran / 4 h / Ambient temperature View Scheme
参考文献
Helvetica Chimica Acta, , vol. 74, # 8 p. 1697 - 1706
反应条件
ammonia; nickel T=205°C;
参考文献
US2412209 , ;
US2357176 , ;
反应条件
1: 88 percent / SOCl2 / 18 h / 80 °C 2: 98 percent / NaN3 3: 92 percent / H2 / Pd View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 9 p. 2672 - 2691
